22990-19-8, 1-Phenyl-1,2,3,4-tetrahydroisoquinoline is a tetrahydroisoquinoline compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
1. 4 will be 43. 63g (0.208mol) 1.3 Phenyl-1,2,3,4-dihydroisoquinoline obtained in the above step (1) was dissolved 305 ml of isopropanol and 130 ml of water,Heated to 70 C, the raw materials completely dissolved,Then, 31. 28 g (0.208 m?) of D-tartaric acid was added,And the reaction temperature 30min, to tartaric acid completely dissolved, stop heating and cooling to room temperature, continue stirring for 3h, a white crystal precipitation, filtration, and washing with isopropanol, the white solid drying at 50 C,(S) -l-phenyl-1,2,3,4-tetrahydroisoquinoline tartrate 32. 75 g, yield 43.7%.
The synthetic route of 22990-19-8 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Jinan Healtang Biotech Co,Ltd; Meng, Qingwen; Wang, Wubao; Zhao, Haifeng; (11 pag.)CN103159677; (2016); B;,
Tetrahydroisoquinoline – Wikipedia
1,2,3,4-Tetrahydroisoquinoline | C9H11N – PubChem