1-Phenyl-1,2,3,4-tetrahydroisoquinoline, cas is 22990-19-8, it is a common heterocyclic compound, the tetrahydroisoquinoline compound, its synthesis route is as follows.
To a reaction flask charged with Pd / C (40 mol% of the substrate in Formula 1), potassium phosphate trihydrate (20 mol% of the substrate in Formula 1) was added 4 ml of acetonitrile in an oxygen atmosphere or in air and stirred at room temperature After a few minutes, 1-phenyl-1,2,3,4-tetrahydroisoquinoline (0. 3 mmol) was added and the reaction was stirred at 60 C for 12-22 hours. Pd / C was filtered and concentrated , And direct column chromatography (eluent: petroleum ether and ethyl acetate = 5: 1 by volume) to give the desired product, 3,4-dihydroisoquinoline, 22990-19-8
With the rapid development of chemical substances, we look forward to future research findings about 1-Phenyl-1,2,3,4-tetrahydroisoquinoline
Reference£º
Patent; Dalian Institute of Chemical Physics, Chinese Academy of Sciences; Zhou, Yonggui; Shi, Lei; Ji, Yue; Chen, Mu Wang; (10 pag.)CN105566218; (2016); A;,
Tetrahydroisoquinoline – Wikipedia
1,2,3,4-Tetrahydroisoquinoline | C9H11N – PubChem