42923-77-3, 6-Methoxy-1,2,3,4-tetrahydroisoquinoline is a tetrahydroisoquinoline compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated,42923-77-3
In a 25 ml round-bottom flask compound is added in 5A (200 mg, 1 . 23mmol), compound 5B (273 mg, 1 . 11mmol), ethyl acetate (2 ml), stirring, add three acetoxy nabh (284 mg, 1 . 34mmol). Stir at room temperature overnight, TLC detection raw material the reaction is complete. Saturated sodium bicarbonate aqueous solution for quenching the reaction, then using ethyl acetate extraction, combined with the organic layer, dry anhydrous sodium sulfate, concentrated after the silica gel column chromatography, with petroleum ether: ethyl acetate (4:1) as eluant, get white solid product 5 (186 mg, yield: 42.7%)
As the paragraph descriping shows that 42923-77-3 is playing an increasingly important role.
Reference£º
Patent; Chengdu Biological Technology Co., Ltd. Kerry Bass; Li, Dequn; (92 pag.)CN105777632; (2016); A;,
Tetrahydroisoquinoline – Wikipedia
1,2,3,4-Tetrahydroisoquinoline | C9H11N – PubChem