Downstream synthetic route of 82771-60-6

82771-60-6,7-Chloro-1,2,3,4-tetrahydroisoquinolinebelongs to tetrahydroisoquinoline compound, is more and more widely used in various fields. and we look forward to future research findings.

82771-60-6,82771-60-6, 7-Chloro-1,2,3,4-tetrahydroisoquinoline is a tetrahydroisoquinoline compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated

The corresponding hydrochloride salt was prepared by addition of a solution of hydrochloric acid gas in isopropyl acetate to the solution of the base (27) in toluene followed by filtration. IR (film): nu?=?3483, 1591, 1486?cm-1. 1H NMR (600?MHz, CD3OD): 7.30 (dd, J?=?8.1, 2.2?Hz, 1H), 7.29 (br s, 1H), 7.25 (d, J?=?8.1?Hz, 1H), 4.35 (br s, 2H), 3.50 (t, J?=?6.4?Hz, 2H), 3.10 (br t, J?=?6.4?Hz, 2H). 13C NMR (150?MHz, CD3OD): 133.7, 131.8, 131.5, 131.3, 129.3, 127.7, 45.4, 42.7, 25.6. HRMS calcd. for C9H11ClN+ ([M+H]+): 168.0575, found: 168.0578.

82771-60-6,7-Chloro-1,2,3,4-tetrahydroisoquinolinebelongs to tetrahydroisoquinoline compound, is more and more widely used in various fields. and we look forward to future research findings.

Reference£º
Article; Hargitai, Csilla; Nagy, Tamas; Halasz, Judit; Kovanyi-Lax, Gyoergyi; Nemeth, Gabor; Simig, Gyula; Volk, Balazs; Tetrahedron; vol. 74; 49; (2018); p. 7009 – 7017;,
Tetrahydroisoquinoline – Wikipedia
1,2,3,4-Tetrahydroisoquinoline | C9H11N – PubChem