42923-79-5, 7-Nitro-1,2,3,4-tetrahydroisoquinoline is a tetrahydroisoquinoline compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated,42923-79-5
7-nitrotetrahydroisoquinoline (35.6 mg, 0.2 mmol), cobalt acetate tetrahydrate (7.5 mg, 0.33 mmol), and a stirrer were placed in a reaction tube. After replacing the inert gas, 1 was added. Dilute DMF and seal the reaction tube. Place the reaction tube in a 150C oil bath and stir the reaction for 3 hours. After cooling to room temperature, dilute with 15 mL of water and extract with ethyl acetate 3 times for 15 mL each. Combine the extracts with anhydrous sodium sulfate. The mixture was dried, filtered, and the filtrate was concentrated under reduced pressure. The crude product was subjected to column chromatography with ethyl acetate:petroleum ether=1:3 (containing 1% triethylamine) as an eluent to obtain a pure product. Brown oil, 75% yield
As the paragraph descriping shows that 42923-79-5 is playing an increasingly important role.
Reference£º
Patent; Xiangtan University; Gong Xing; Xie Guilin; Cai Changqun; Ma Juan; (21 pag.)CN107892670; (2018); A;,
Tetrahydroisoquinoline – Wikipedia
1,2,3,4-Tetrahydroisoquinoline | C9H11N – PubChem